Sediments from the anoxic center (ca. 590m water depth; 34¡14'N;120¡01'W) of the Santa Barbara Basin were collected in February, 1988 during a sampling cruise (SABA 88-1) aboard the Scripps Institution of Oceanography vessel the R.V. Sproul . Continuous sediment sequences from multiple stations within the basin were collected over several days. The sediments were retrieved using a Soutar-style box corer (Soutar & Crill, 1977). Upon retrieval, the sediment surface was examined for disturbance and only those cores which showed no apparent disruption of the surface layer were considered and examined. Subsampling of the box core with limited disturbance of the laminae was achieved using an acrylic core liner (8.3 cm i.d.) beveled on one end for clean penetration. Application of a carefully controlled vacuum on the top of the core liner allows insertion while maintaining a comparable level for the sediment water interface both inside and outside of the core liner, and thereby avoids disruption of the laminae (Schimmelmann et al., 1990). Three cores were collected in this manner for this study. Two (10a,10b) were subsampled from within the same box core, a few centimeters apart, and the third (9) was taken from an immediately adjacent box core recovered at the same station site. Cores 9 and 10b were capped, labeled and transferred to refrigerated storage aboard ship, and were held in cold storage in the core repository at SIO until subsampling in March, 1990. Subsampling of core 10a was started while aboard ship and completed at SIO. The procedures utilized for fine-scale subsampling of cylindrical cores were developed at SIO and are fully described by Schimmelmann et al (1990). In their technique, the core liner is mounted onto a plunger with a diameter approximately equal to that of the core liner. The acrylic tube and plunger are firmly affixed to a countertop in an upright position via a wall bracket. The plunger is forced upward a known distance (3.19mm) by each rotation of a worm gear. The sediment in the core liner is forced upward until the core surface is even with the lip of the core liner, establishing a baseline or zero position. The color of the surface layer is described using a Munsell soil color chart (5Y), and other unusual features are noted such as the presence of wood or shell fragments, small gastropods or foraminifera (Appendix A.1). The uniformly colored layer is removed to a clean, weighed, plastic sample bag by careful scraping with a stainless steel spatula until underlying sediment of a differing color can be seen. The plunger is then driven upward an appropriate number of rotations to bring the new surface layer level with the lip of the core liner, back to the zero position. The number of rotations enables calculation of the subsurface depth of all individually described laminae. Somewhat contrary to their general description as a sequence of alternating light and dark layers, the SBB cores are not bimodal in their color distribution. Individual layers range from black to various shades of gray, green-gray, olive green, and yellow (Appendix A.1). Such layers may range in thickness from 1-2 millimeters (generally very black or yellow sediments) to several millimeters (frequently gray to olive green layers). Where possible, the carefully removed subsamples constituted individual layers of a uniform color. However, due to the significant cohesive strength between the layers, many samples include small portions of underlying and/or overlying layers. Those layers of uniform color which extended over several millimeters were generally split for ease of subsequent analytical workup. The average sample thickness collected was approximately 3mm. Immediately after subsampling, wet sediments were heat-sealed (1 to 2 seconds in a "seal a meal"-type sealing device) in the plastic sample bags and then frozen. Sample weights were taken as frozen wet weights (Appendix A.2). Cores 10a and 10b were transported frozen to Stanford and held in freezer storage until subsequent work-up. Samples from core 9 were freeze- dried over a period of 3 days at SIO using a freeze drying system designed and built by Dr. Arndt Schimmelmann. Dry weights were then taken for calculation of pore fluid content (Appendix A.2), aiding correlation to SIO stratigraphic age assignments determined on previously collected cores. Stratigraphic Correlation of Santa Barbara Basin Cores Of the three cores collected from the SBB, core 10a consisted of 178 samples, of which 100 were extracted and analyzed. 100 subsamples were taken from cores 10b and 9, of which 35 and 30 were analyzed, respectively. All unprocessed, nonfreeze-dried subsamples remain in freezer storage. Assignment of stratigraphic ages for all samples in these cores was ultimately to be based on comparison with published stratigraphic age assignments (Schimmelmann et al., 1990; many stratigraphic assignments based on more detailed unpublished results provided by A. Schimmelmann), utilizing subsurface depths and the pore fluid content of individual samples in core 9. Inherent in the correlation is the assumption that the physical characteristics of equivalent, individual layers are spatially consistent over the distances separating the cores, at most a few meters for core 9 and a few centimeters for cores 10a and 10b. The subsurface depth assignments recorded for core 10a are not viewed with high confidence here, because of inexperience with the sampling technique and also jostling of the core during transport from the ship to the SIO lab midway through the subsampling process. However, the sampling of cores 9 and 10b, conducted on successive days in March of 1990, are viewed with greater confidence. As the pore fluid content was only applicable to core 9, and accurate subsurface depths were unavailable for 10a, the equivalency between cores 9, 10a and 10b needed to be established by alternate criteria. The extracts of surface samples from all cores were analyzed for their alkenone unsaturation profiles and the profiles compared. The subsurface depths (and therefore the timing) of positive excursions seen in the profiles coincided well for cores 10a and 10b, but similar excursions in core 9 lagged, appearing approximately 8mm deeper in the core. This lag most probably can be attributed to the absence of the uppermost surface in the box core from which subcores 10a and 10b were collected, despite the lack of discernible disturbance to the surface of the core. Such loss can occur during the initial coring process and may not necessarily be visually evident, as the fluff layer which characterizes the surface can be 1-2cm thick. Alternative explanations such as nondeposition or local variability in the stratigraphic sequence are precluded by the close physical spacing of all cores (within a few meters); a distance over which sedimentological and molecular variability is unlikely. Therefore the records for cores 10a and 10b were shifted downwards by 8mm to become in phase with that of core 9. To confirm that the excursions in core 9 and those in 10a and 10b were equivalent events, the absolute distance in sediment depth between several excursions in the upper 5cm was calculated for all three cores and their values compared. The coincidence of depth differences between individual excursions confirmed that the three cores were all recording the events simultaneously, and that the uppermost 8mm of cores 10a and 10b had not been recovered in the coring process. Final sediment depths for these cores were therefore adjusted appropriately. The wet (frozen) weights of the individual samples were used to establish absolute correspondence between the cores for all depths. The equivalent mass of the 8mm of sediment missing from cores 10a and 10b was calculated from the wet weight of the upper 8mm of sediment in core 9. The wet weights (minus the weight of the empty sample bag) off all samples from each of the cores were successively summed, so that the total wet mass overlying any given depth in the sediment column could be found (Appendix A.3). The weight of the missing mass was then added to the summed values for cores 10a and 10b. Correspondence between the cores was then established on the basis that, because of the mutual proximity of the cores and the overall uniformity of sedimentary conditions in the central basin, equivalent layers from among the cores would be overlain by equivalent wet masses. Correspondence of accumulated masses, therefore, gave equivalence of layers. This technique allowed a depth profile to be established for core 10a from measured core 9 depth values. Pore fluid contents and subsurface depths for core 9 were compared to those of Schimmelmann et al. (1990 and unpublished results), and ages adopted accordingly. The depths of individual layers with characteristically high or low pore fluid contents were independently compared with the depths of the presumably equivalent SIO layers, and were found to be in agreement to within a few millimeters. This confirmed the more accurate subsampling technique employed during the later sampling interval. Ages established in this manner for layers within core 9 were adopted for the mass-equivalent layers in core 10a.