Sclerosponge Minor Element Data ----------------------------------------------------------------------- World Data Center for Paleoclimatology, Boulder and NOAA Paleoclimatology Program ----------------------------------------------------------------------- NOTE: PLEASE CITE CONTRIBUTORS WHEN USING THIS DATA!!!!! NAME OF DATA SET: Sclerosponge Minor Element Data LAST UPDATE: 11/2005 (Original receipt by WDC Paleo) CONTRIBUTOR: Brad Rosenheim, Woods Hole Oceanographic Institution IGBP PAGES/WDCA CONTRIBUTION SERIES NUMBER: 2005-080 SUGGESTED DATA CITATION: Rosenheim, B.E., et al. 2005. Sclerosponge Minor Element Data. IGBP PAGES/World Data Center for Paleoclimatology Data Contribution Series # 2005-080. NOAA/NCDC Paleoclimatology Program, Boulder CO, USA. ORIGINAL REFERENCE: Rosenheim, B.E., P.K. Swart, and S.R. Thorrold. 2005. Minor and trace elements in sclerosponge Ceratoporella nicholsoni: Biogenic aragonite near the inorganic endmember? Palaeogeography, Palaeoclimatology, Palaeoecology, Vol. 228, Issues 1-2, 22 November 2005, Pages 109-129, doi:10.1016/j.palaeo.2005.03.055 ABSTRACT: The trace and minor element composition have been investigated in the accretionary skeletons of two specimens of the Caribbean sclerosponge species, Ceratoporella nicholsoni; one from Tongue of the Ocean, Bahamas (TOTO), and the other from Pear Tree Bottom, Jamaica (PTB). Both sclerosponges were analyzed at high resolution using laser ablation ICP-MS (LA-ICP-MS) and verified using wet chemical methods (ICP-OES). The shallow PTB sclerosponge (25 m) was analyzed for a short, temperature-calibrated record of trace and minor elements while the TOTO sclerosponge (146 m) was analyzed for a century long record from subsurface waters. The resulting Ba/Ca, Mg/Ca, Pb/Ca, and U/Ca ratios were compared with Sr/Ca ratios, which have been shown to reliably record seasonal-scale temperature change in sclerosponges, close to equilibrium precipitation of inorganic aragonite. Sclerosponge aragonite incorporates minor and trace elements according to general mineralogic constraints with less "vital" effects than other calcium carbonate secreting organisms. This is perhaps most obvious in the behavior of Mg/Ca ratios which show an inverse correlation to temperature unlike any other calcite or aragonite organism, despite having Mg concentrations (~1 mmol/mol) within published estimates of equilibrium aragonite. Ratios of Mg/Ca and Ba/Ca show a strong positive correlation despite large differences in ionic radii and U/Ca values (~3.15 Mmol/mol) are 2.5× higher in sclerosponge aragonite than in aragonite from corals, supporting earlier work. Ratios of U/Ca show an insignificant correlation with temperature-dependent Sr/Ca ratios (r2 = 0.05), supporting existing theories that temperature signals recorded by U/Ca ratios can be convolved with pH, [CO3-2], and phosphate signals. Differences between sclerosponge aragonite and other calcium carbonate arising from siliceous spicule contamination are unlikely because of the small mole percent of silicon in the aragonite. Small differences between the two sclerosponges were noticed in Pb/Ca and Sr/Ca because of the average ages of the sampled material and average temperatures of the ambient environment, respectively. Anomalies between LA-ICP-MS and ICP-OES were noticed in measurements of Ba/Ca and Pb/Ca due to standardization differences for LA-ICP-MS (Ba/Ca) and measurements close to the instrument detection limits of Pb (ICP-OES). GEOGRAPHIC REGION: Tropical Atlantic/Caribbean Sea PERIOD OF RECORD: 1890-1990 AD DESCRIPTION: Sclerosponge minor element records from Tongue of the Ocean (TOTO), one of the Bahamas' deep channels, and Pear Tree Bottom (PTB), Jamaica. Samples: Sclerosponge Ceratoporella nicholsoni taken from water depths of 143 m (Tongue of the Ocean (TOTO) and 25 m. (PTB) Pear Tree Bottom, Jamaica sclerosponge minor element data: Raw data, as published, correlated with a temperature measured adjacent to the sclerosponge in degrees Celsius. Tongue of the Ocean, Bahamas sclerosponge minor element data: Raw data, as published, correlated with a distance in the sclerosponge skeleton (mm). DATA: 1. Jamaica sclerosponge minor element data Temp. Ba/Ca Mg/Ca Pb/Ca Sr/Ca U/Ca oC (umol/mol) (mmol/mol) (nmol/mol) (mmol/mol) (umol/mol) 28.46562514 1.282060692 0.910679201 110.5754492 9.724481472 3.282835845 29.14171293 1.285227482 0.878434124 91.85105967 9.519879984 3.23629749 28.44987335 1.266288784 0.889114976 92.5445632 9.620906181 3.223044339 27.92745556 1.277086104 0.900740087 94.02301408 9.750025974 3.234241563 27.1761038 1.274912531 0.896373476 98.28197505 9.775784414 3.206770705 26.61958448 1.301803622 0.896274211 98.29349855 9.821479925 3.197347518 26.40072649 1.332159417 0.911783067 98.9225888 9.890581998 3.213564561 26.4016219 1.338810346 0.915764257 98.11248597 9.860426265 3.219076015 26.89260904 1.338978484 0.91014325 96.62422797 9.854879033 3.238583744 27.41801461 1.293869521 0.8829778 99.42887359 9.691932731 3.258973625 28.00075373 1.259420301 0.865428366 100.4099615 9.55161675 3.291264847 28.28999552 1.270896036 0.867887309 98.15114013 9.556383443 3.311909947 28.87688988 1.272419148 0.862524385 100.5786585 9.480910963 3.297968438 28.99379027 1.2647888 0.860623096 103.3322793 9.449911216 3.310937053 28.2098868 1.248011532 0.853021196 101.7801798 9.461051022 3.334686382 27.37130619 1.267260128 0.856036829 108.2842765 9.54633134 3.29977281 26.41478035 1.319389297 0.874910806 115.5200794 9.709616656 3.259674322 25.9905108 1.36636503 0.896550073 119.8124149 9.843456077 3.225908143 26.7288815 1.323946021 0.889509834 117.5378559 9.701202795 3.290709336 28.81968502 1.26888131 0.881757921 111.3834148 9.552491472 3.365002751 29.65154347 1.246382905 0.882513753 108.1837766 9.513100814 3.358289697 2. TOTO sclerosponge minor element data Dist. Sr/Ca Mg/Ca Ba/Ca Pb/Ca U/Ca mm. (mmol/mol) (mol/mol) (mol/mol) (mol/mol) (mol/mol) 0.1 10.32794405 0.001050958 3.68E-06 2.59E-07 3.75E-06 0.12 10.44042574 0.001011547 3.86E-06 2.71E-07 3.46E-06 0.14 10.31269304 0.000955092 3.80E-06 2.18E-07 3.58E-06 0.16 10.14843734 0.00086199 3.59E-06 1.75E-07 3.41E-06 0.18 9.874259654 0.000842741 3.52E-06 1.68E-07 3.28E-06 0.2 9.983965977 0.000875063 3.60E-06 1.62E-07 3.19E-06 0.22 9.94813954 0.000885901 3.72E-06 1.66E-07 3.10E-06 0.24 10.00535027 0.000882496 3.52E-06 1.64E-07 3.17E-06 0.26 9.843913489 0.000851733 3.48E-06 1.84E-07 3.08E-06 0.28 10.17100948 0.000897027 3.62E-06 1.86E-07 3.17E-06 0.3 10.23479293 0.000893769 3.54E-06 2.02E-07 3.13E-06 0.32 10.32697009 0.000916108 3.80E-06 2.00E-07 3.28E-06 0.34 10.37369284 0.000966215 3.72E-06 2.00E-07 3.21E-06 0.36 10.03318885 0.000952056 3.67E-06 1.82E-07 3.21E-06 0.38 10.19069264 0.000896118 3.61E-06 2.10E-07 3.39E-06 0.4 10.28726888 0.000932568 3.66E-06 2.15E-07 3.37E-06 0.42 10.52231027 0.000912053 3.66E-06 1.66E-07 3.42E-06 0.44 10.74082602 0.000846943 3.96E-06 1.77E-07 3.45E-06 0.46 10.19703234 0.000834091 3.61E-06 1.71E-07 3.21E-06 0.48 10.54824277 0.000906737 3.67E-06 1.61E-07 3.43E-06 0.5 10.28888414 0.000851492 3.52E-06 1.44E-07 3.17E-06 0.52 10.23103096 0.000893262 3.87E-06 1.53E-07 3.51E-06 0.54 10.27732805 0.000881324 3.69E-06 1.45E-07 3.21E-06 0.56 10.37334852 0.000890268 3.69E-06 1.41E-07 3.26E-06 0.58 9.921350977 0.000857422 3.57E-06 1.40E-07 3.45E-06 0.6 10.01901255 0.000874599 3.45E-06 1.45E-07 3.42E-06 0.62 10.10902551 0.000872933 3.71E-06 1.57E-07 3.43E-06 0.64 10.5391411 0.000855247 3.63E-06 1.74E-07 3.43E-06 0.66 10.67137554 0.000928043 3.89E-06 2.06E-07 3.43E-06 0.68 10.46558306 0.00090727 3.82E-06 2.02E-07 3.50E-06 0.7 10.50280225 0.000973479 3.82E-06 2.20E-07 3.17E-06 0.72 10.45173858 0.00091318 3.78E-06 2.22E-07 3.31E-06 0.74 9.96473441 0.000897106 3.58E-06 2.08E-07 3.08E-06 0.76 10.15054739 0.000904083 3.67E-06 2.21E-07 3.12E-06 0.78 10.50463573 0.000991343 3.89E-06 2.48E-07 3.16E-06 0.8 10.44586117 0.001017341 4.06E-06 2.59E-07 3.22E-06 0.82 10.67370826 0.000956891 4.01E-06 2.66E-07 3.39E-06 0.84 10.65031865 0.000955748 4.08E-06 2.75E-07 3.31E-06 0.86 10.42688398 0.000914278 3.77E-06 2.33E-07 3.21E-06 0.88 10.57597976 0.000912525 3.77E-06 2.32E-07 3.22E-06 0.9 10.52838974 0.000945245 3.93E-06 2.42E-07 3.15E-06 0.92 10.36036656 0.000918173 3.90E-06 2.46E-07 3.23E-06 0.94 10.83541085 0.000953065 4.16E-06 2.46E-07 3.19E-06 0.96 10.94217053 0.000920511 3.98E-06 2.13E-07 3.28E-06 0.98 10.23529719 0.000871247 3.79E-06 1.63E-07 3.17E-06 1 10.44955734 0.00087248 3.95E-06 2.09E-07 3.08E-06 1.02 10.56659135 0.000888667 3.93E-06 2.18E-07 3.12E-06 1.04 10.38966656 0.000878211 3.89E-06 2.12E-07 3.14E-06 1.06 10.35922953 0.000864024 3.86E-06 2.20E-07 3.21E-06 1.08 10.59481215 0.000873609 3.89E-06 2.27E-07 3.22E-06 1.1 10.54033849 0.000862217 3.88E-06 2.07E-07 3.12E-06 1.12 10.53003432 0.000875766 3.92E-06 2.02E-07 3.08E-06 1.14 10.69054116 0.000887589 4.02E-06 2.06E-07 3.13E-06 1.16 10.64969832 0.000836321 4.05E-06 2.04E-07 3.11E-06 1.18 10.53776779 0.00083734 3.95E-06 1.83E-07 3.17E-06 1.2 10.36773559 0.00081583 3.81E-06 1.52E-07 3.22E-06 1.22 10.35996803 0.000832323 3.72E-06 1.73E-07 3.12E-06 1.24 10.13798099 0.000787424 3.60E-06 1.57E-07 3.20E-06 1.26 10.10751159 0.000807463 3.61E-06 1.63E-07 3.13E-06 1.28 10.37234918 0.000788034 3.52E-06 1.49E-07 3.24E-06 1.3 10.2968399 0.000797254 3.50E-06 2.28E-07 3.29E-06 1.32 10.32645234 0.000831499 3.60E-06 2.24E-07 3.31E-06 1.34 10.38136512 0.000854997 3.64E-06 2.24E-07 3.34E-06 1.36 10.42182082 0.000849859 3.63E-06 2.34E-07 3.22E-06 1.38 10.91010811 0.000874038 3.64E-06 2.54E-07 3.31E-06 1.4 10.45876005 0.000880678 3.78E-06 2.54E-07 3.37E-06 1.42 10.62913538 0.000894319 3.66E-06 2.75E-07 3.22E-06 1.44 10.52734238 0.0008535 3.75E-06 3.03E-07 3.28E-06 1.46 10.89273744 0.000889698 3.72E-06 2.75E-07 3.44E-06 1.48 10.04467077 0.00080823 3.50E-06 2.74E-07 3.45E-06 1.5 10.54488548 0.000815187 3.63E-06 2.70E-07 3.37E-06 1.52 10.50504693 0.000817442 3.55E-06 2.46E-07 3.41E-06 1.54 9.919861506 0.000781065 3.46E-06 2.33E-07 3.27E-06 1.56 10.60377896 0.00086198 3.70E-06 2.53E-07 3.35E-06 1.58 10.41443082 0.000828761 3.41E-06 2.59E-07 3.32E-06 1.6 10.0758056 0.000823201 3.24E-06 2.74E-07 3.33E-06 1.62 10.51589673 0.000894871 3.71E-06 3.28E-07 3.29E-06 1.64 9.912697604 0.000833099 3.46E-06 3.10E-07 3.10E-06 1.66 9.927713509 0.000830396 3.42E-06 3.14E-07 3.29E-06 1.68 10.50094854 0.000869686 3.51E-06 3.22E-07 3.21E-06 1.7 10.64684119 0.00087541 3.49E-06 3.05E-07 3.25E-06 1.72 10.70462246 0.000893764 3.61E-06 3.34E-07 3.16E-06 1.74 10.28540404 0.000816461 3.32E-06 3.00E-07 3.24E-06 1.76 10.31315943 0.000801927 3.39E-06 2.74E-07 3.49E-06 1.78 10.72880587 0.000855733 3.59E-06 2.90E-07 3.39E-06 1.8 10.43313365 0.000834285 3.54E-06 2.85E-07 3.33E-06 1.82 10.37423518 0.000812138 3.43E-06 2.47E-07 3.33E-06 1.84 9.963940039 0.000834485 3.35E-06 2.17E-07 3.17E-06 1.86 9.71508844 0.000757328 3.01E-06 2.02E-07 3.13E-06 1.88 10.30069476 0.000829398 3.25E-06 1.97E-07 3.21E-06 1.9 10.19390993 0.000752975 3.17E-06 2.00E-07 3.04E-06 1.92 10.17006787 0.000805773 3.14E-06 1.83E-07 3.20E-06 1.94 10.26286798 0.000744534 3.08E-06 1.81E-07 3.29E-06 1.96 10.69501392 0.000790472 3.21E-06 1.92E-07 3.31E-06 1.98 10.25745254 0.000743407 3.09E-06 1.96E-07 3.22E-06 2 9.988635595 0.000703732 3.06E-06 2.10E-07 3.23E-06 2.02 10.5409462 0.000716835 2.97E-06 2.00E-07 3.06E-06 2.04 9.919421633 0.000676456 2.91E-06 1.70E-07 3.03E-06 2.06 10.73056836 0.000762209 3.22E-06 1.94E-07 3.19E-06 2.08 10.10672958 0.000718183 3.02E-06 1.96E-07 3.07E-06 2.1 10.4763627 0.000737765 3.23E-06 1.99E-07 3.13E-06 2.12 9.984280475 0.000750641 3.24E-06 2.39E-07 3.14E-06 2.14 10.26877393 0.000795129 3.19E-06 2.58E-07 3.12E-06 2.16 10.36376518 0.000818467 3.30E-06 2.94E-07 3.12E-06 2.18 10.32479309 0.000839121 3.44E-06 3.53E-07 3.06E-06 2.2 10.80066376 0.000909245 3.78E-06 4.44E-07 3.25E-06 2.22 10.88078174 0.000882205 3.88E-06 5.01E-07 3.14E-06 2.24 10.51323125 0.000866055 3.81E-06 5.14E-07 3.34E-06 2.26 10.64171877 0.000835728 3.71E-06 5.20E-07 3.31E-06 2.28 10.56732983 0.000847894 3.66E-06 4.40E-07 3.32E-06 2.3 10.66391591 0.000851948 3.76E-06 4.54E-07 3.23E-06 2.32 10.29238237 0.000867934 3.68E-06 4.47E-07 3.37E-06 2.34 10.35246778 0.000855811 3.71E-06 4.10E-07 3.17E-06 2.36 10.30155172 0.00084417 3.77E-06 3.91E-07 3.24E-06 2.38 10.1624486 0.000819166 3.55E-06 4.04E-07 3.17E-06 2.4 10.36270216 0.000826302 3.64E-06 3.54E-07 3.36E-06 2.42 10.78139302 0.000850841 3.65E-06 3.50E-07 3.34E-06 2.44 10.72762558 0.000828595 3.62E-06 3.46E-07 3.33E-06 2.46 10.65223734 0.000829806 3.55E-06 3.65E-07 3.39E-06 2.48 9.977276506 0.000829777 3.54E-06 3.56E-07 3.23E-06 2.5 10.18903339 0.000823504 3.31E-06 2.98E-07 3.28E-06 2.52 10.13600558 0.000824775 3.46E-06 3.35E-07 3.21E-06 2.54 10.48913368 0.000841753 3.50E-06 3.46E-07 3.23E-06 2.56 10.52731616 0.000891199 3.65E-06 3.92E-07 3.28E-06 2.58 10.42561568 0.000847169 3.63E-06 3.60E-07 3.17E-06 2.6 9.957249386 0.000858979 3.48E-06 3.79E-07 3.19E-06 2.62 10.42502936 0.000877291 3.61E-06 4.05E-07 3.13E-06 2.64 10.68356401 0.000891251 3.84E-06 4.39E-07 3.13E-06 2.66 10.73416218 0.000928552 3.73E-06 4.41E-07 3.03E-06 2.68 10.55286029 0.000915464 3.83E-06 4.32E-07 3.14E-06 2.7 10.646805 0.000918671 3.81E-06 4.62E-07 3.11E-06 2.72 10.70436412 0.000885888 3.66E-06 4.45E-07 3.07E-06 2.74 10.5904893 0.000902667 3.81E-06 4.42E-07 3.28E-06 2.76 10.46065755 0.000864889 3.70E-06 4.20E-07 3.29E-06 2.78 10.49923463 0.000840127 3.55E-06 3.99E-07 3.29E-06 2.8 10.25232224 0.000810005 3.47E-06 3.95E-07 3.20E-06 2.82 10.25506877 0.000780138 3.32E-06 4.11E-07 3.22E-06 2.84 10.24749181 0.000802203 3.29E-06 3.95E-07 3.22E-06 2.86 10.21007452 0.00077334 3.33E-06 3.69E-07 3.32E-06 2.88 10.06872455 0.000799829 3.19E-06 3.61E-07 3.29E-06 2.9 10.42398131 0.000801498 3.29E-06 3.82E-07 3.39E-06 2.92 9.867071665 0.000746876 3.10E-06 3.42E-07 3.29E-06 2.94 10.34264334 0.000765957 3.13E-06 3.60E-07 3.38E-06 2.96 9.980658367 0.00068822 2.97E-06 3.36E-07 3.23E-06 2.98 10.04827173 0.00070709 3.04E-06 3.44E-07 3.21E-06 3 10.26478552 0.000745853 3.16E-06 3.37E-07 3.43E-06 3.02 9.864987059 0.000718503 3.07E-06 3.23E-07 3.23E-06 3.04 10.24965369 0.000684124 2.97E-06 3.23E-07 3.05E-06 3.06 10.11177619 0.000715742 3.03E-06 3.26E-07 3.16E-06 3.08 10.33727819 0.000750851 3.05E-06 3.29E-07 3.27E-06 3.1 10.22561754 0.000729786 3.01E-06 3.05E-07 3.17E-06 3.12 10.50149278 0.000738644 3.02E-06 3.05E-07 3.18E-06 3.14 10.2628969 0.000716164 3.09E-06 3.34E-07 3.22E-06 3.16 10.38422096 0.000777363 3.28E-06 3.59E-07 3.45E-06 3.18 10.09300367 0.000794674 3.21E-06 3.68E-07 3.35E-06 3.2 10.60420747 0.000860035 3.61E-06 4.05E-07 3.42E-06 3.22 10.00655997 0.000810227 3.34E-06 3.85E-07 3.07E-06 3.24 10.51003311 0.000839821 3.44E-06 4.37E-07 3.26E-06 3.26 10.15219922 0.000845159 3.51E-06 4.84E-07 3.19E-06 3.28 10.71818749 0.000873602 3.60E-06 5.03E-07 3.24E-06 3.3 10.70712837 0.000918123 3.71E-06 5.26E-07 3.12E-06 3.32 10.41062782 0.000885096 3.68E-06 5.50E-07 3.11E-06 3.34 10.62331566 0.000902325 3.71E-06 5.46E-07 2.99E-06 3.36 10.64229784 0.00090994 3.76E-06 5.20E-07 3.16E-06 3.38 10.50004304 0.000882736 3.66E-06 4.91E-07 3.22E-06 3.4 9.927839319 0.000812348 3.48E-06 4.66E-07 3.09E-06 3.42 10.51438454 0.000833489 3.50E-06 4.75E-07 3.26E-06 3.44 10.25955792 0.000843583 3.43E-06 4.70E-07 3.20E-06 3.46 10.21072585 0.000869051 3.52E-06 4.46E-07 3.27E-06 3.48 10.54661677 0.000836523 3.46E-06 4.50E-07 3.25E-06 3.5 10.71639709 0.000805397 3.47E-06 4.31E-07 3.28E-06 3.52 10.56819328 0.000834855 3.47E-06 4.41E-07 3.14E-06 3.54 10.55222199 0.000829996 3.44E-06 4.36E-07 3.17E-06 3.56 10.0675169 0.000783066 3.37E-06 4.05E-07 3.17E-06 3.58 10.65688138 0.000806074 3.48E-06 3.91E-07 3.26E-06 3.6 10.16730751 0.000788819 3.18E-06 3.76E-07 3.18E-06 3.62 10.56366946 0.000785799 3.33E-06 3.99E-07 3.32E-06 3.64 10.34356944 0.000773002 3.18E-06 3.74E-07 3.24E-06 3.66 10.16861165 0.000779192 3.27E-06 3.86E-07 3.14E-06 3.68 9.997484895 0.000757166 3.16E-06 3.54E-07 3.32E-06 3.7 9.96440909 0.000772851 3.18E-06 3.31E-07 3.26E-06 3.72 10.05670591 0.000794828 3.33E-06 3.55E-07 3.29E-06 3.74 10.36987721 0.000811232 3.43E-06 3.38E-07 3.34E-06 3.76 10.32249221 0.000828948 3.41E-06 3.41E-07 3.40E-06 3.78 10.09638738 0.000800241 3.20E-06 3.23E-07 3.24E-06 3.8 9.981329051 0.000808192 3.25E-06 3.18E-07 3.34E-06 3.82 10.16513325 0.000825287 3.29E-06 3.38E-07 3.25E-06 3.84 10.39186976 0.000842528 3.49E-06 3.38E-07 3.27E-06 3.86 10.51523054 0.000848737 3.40E-06 3.64E-07 3.33E-06 3.88 10.57426434 0.000863032 3.46E-06 3.73E-07 3.37E-06 3.9 10.2614473 0.000829795 3.36E-06 3.94E-07 3.25E-06 3.92 10.17812632 0.000849522 3.31E-06 4.19E-07 3.19E-06 3.94 10.75611442 0.000871899 3.64E-06 4.29E-07 3.30E-06 3.96 10.56489126 0.000896569 3.59E-06 4.46E-07 3.16E-06 3.98 10.42032274 0.000889173 3.60E-06 4.53E-07 3.11E-06 4 10.30149829 0.000883601 3.51E-06 4.73E-07 3.02E-06 4.02 10.956801 0.000909487 3.83E-06 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